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A double-blind, randomised, placebo-controlled trial of Ganoderma lucidum for the treatment of cardiovascular risk factors of metabolic syndrome

mobile phase is the triethylamine buffer solution (8ml of phosphate, 15ml of triethylene amine, 1500ml of water, pH adjusted to 5.4) - tetrahydrofuran(THF) mixture, the time gradient is listed in the following Table 2: Table 2 HPLC gradient time table Time(min) Triethylamine buffer solution (%) THF (%) 0 75 25 10 75 25 11 30 70 18 30 70 19 75 25 25 75 25 Step 1 Preparation of L-3-chloro-2-hydroxypropyl trimethylammonium Firstly, the content of L-isomer of S-epichlorohydrin was detected according to the method of example 1 above

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10.3390/ijms24065705 230 ZhangP.JiangY.YeX.ZhangC.TangY

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